DOI码：10.1016/j.mtcomm.2022.104955
发表刊物：Materials Today Communications
关键字：Wet chemical method, W-Re alloy, SPS, Reduction temperature
摘要：Tungsten-rhenium (W-10Re) powder was successfully prepared by wet chemistry method followed by spark plasma sintering technique to fabricate W-10Re alloy. The synthesis mechanism and reduction behavior of the W- 10Re powders were investigated by using X-ray diffraction (XRD), thermogravimetric experiments, and X-ray photoelectron spectroscopy. The reduction process of W-10Re powders from 100 ◦C to 1200 ◦C was divided into four stages, and the optimal reduction temperature region is 1000–1100 ◦C. The reduced powders with irregular cube-shape were examined by transmission electron microscope. The XRD results of powders reduced at 1000–1200 ◦C showed an overall right shift with the increase in temperature, indicating the solid solution of Re into W. The microstructure and mechanical properties of the alloys were studied using XRD, transmission electron microscopy, scanning electron microscopy, and Vickers hardness. The relative densities and grain sizes were comparable for the W-10Re alloys prepared from the powders reduced at 1000 ◦C, 1100 ◦C, and 1200 ◦C, whereas the Vickers hardness was decreased with the increase in the reduction temperature for those samples. The characterization of fracture toughness for these W-10Re alloys showed largely intergranular fracture with a small number of transgranular features.
第一作者：Wang-zhi Xu
论文类型：期刊论文
通讯作者：Lai-ma Luo,Jing Wang
论文编号：104955
学科门类：工学
期号：34
是否译文：否
发表时间：2022-11-15
收录刊物：SCI